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Article Dans Une Revue Journal of Nanoparticle Research Année : 2020

An intercomparison exercise of good laboratory practices for nano-aerosols size measurements by mobility spectrometers

Résumé

An intercomparison campaign on nanoparticle size measurement was organized in the frame of the French nanoMetrology club. The aim of this study is to make an inventory of the metrological capabilities of all measurement techniques in France involved in the “nano” size range, including the SMPS (Scanning Mobility Particle Sizer) concerning aerosol metrology. For this study, four samples have been proposed, namely (1) - a SiO2 colloidal suspension (FD304) consisting of a monomodal population, (2) - two samples consisting of two nanoparticle populations of SiO2 having proportions to be determined and (3) - a TiO2 colloidal suspension. Ten SMPS associated to five participants around a common experimental setup were performed in link with a control SMPS to have simultaneous measurements with a same instrument in each laboratory in parallel with the SMPS used by each partner. This article presents SMPS results of this study associated with the description of the experimental set-up and the sample preparation protocol with an identified schedule and comparison with SEM measurements. The present paper does not focus on the actual capability of the tested mobility spectrometers, but aims to highlights the good laboratory practices using their own but common resources in terms of aerosol generation and measurement set-ups.
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Dates et versions

hal-03118130 , version 1 (21-01-2021)

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Citer

F. Gaie-Levrel, Sébastien Bau, Lola Bregonzio-Rozier, Romain Payet, Sébastien Artous, et al.. An intercomparison exercise of good laboratory practices for nano-aerosols size measurements by mobility spectrometers. Journal of Nanoparticle Research, 2020, 22 (103), pp.103. ⟨10.1007/s11051-020-04820-y⟩. ⟨hal-03118130⟩
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